Downloadable HPLC Troubleshooting
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Downloadable HPLC Troubleshooting
From MACHEREY-NAGEL Inc.
Content:
chapter 1
broad peaks
fronting
tailing
chapter 2
double peaks
negative peaks
spikes
ghost peaks
chapter 3
lack of sensitivity
poor sample recovery
high back pressure
chapter 4
fluctuating pressure
increasing pressure
decreasing pressure
basisline drift to high absorption
basisline drift to low absorption
ondulating baseline
chapter 5
baseline noise
baseline noise during gradient elution or isocratic proportion
disturbance at dead time
leaks
decreasing retention time
increasing retention time
fluctuating retention time
fluctuating retention time from insufficient equilibration
Last update 14-Dec-2005, Rating Very Good of 17 votes.
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i got over sound at pump head: what is the problem
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first you check the filter is it dip in bottle or not? and another is your filter containing air bubble so sonicate your filter in methanol.
Rating: Excellent!
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Not able to open this document. Has it been removed. Have problems with baseline in gradient elution. Baseline goes down as buffer B (50% AcN) is increased????
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Is it possible to go derivatisation in hplc by using PDA detector
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explain the involvement of ion-pair reagent in HPLC analysis
Rating: Good
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I am getting an error message as solvent is too low.byt my solvent is full in the bottle can somebody help me
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I woild lile to get the details of all Item, May I know ,can I get all above informations?, very appreciate for your suggestion
Rating: Excellent!
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Excellent. Very informative.
Rating: Excellent!
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how to eliminate some problems
noise in baseline
rise in pressure
fluctuation in baseline
rise in pressure
Rating: Fair
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very informative thanks
Rating: Excellent!
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very informative thanks
Rating: Very Good
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very informative and easy to understand
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more informative
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most valuable
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This is very very good for those who are at learning stage.
Rating: Excellent!
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thios basic information is breath for me to continue my work on HPLC
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informative
Rating: Excellent!
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